HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1,3-propanediol → 2-(((12-Chloro-6-chrysenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| Reactant | 12-Chloro-6-chrysenecarbaldehyde | HCID 13375389 | — |
| Reactant | 2-((6-Chrysenylmethyl)amino)-2-methyl-1,3-propanediol methanesulfonate | HCID 54096087 | — |
| Product | 2-(((12-Chloro-6-chrysenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate | HCID 131715423 | — |
Reaction Steps
Using the reductive amination procedure outlined in 1C, 12-chloro-6-chrysenecarbaldehyde (4A) and 2-amino-2-methyl-1,3-propanediol (Aldrich) gave 2-(((12-chloro-6-chrysenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate.1/3H2O mp 233°-233.5° (dec), (EtOH/Et2O), (C,H,Cl,N,S).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04810727 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-50353f8b43f24599a1d0bce080869455 |
| Source note | uspto-grants-1989_03 |