HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1,3-propanediol → 2-(((12-Ethyl-6-chrysenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| Reactant | 12-Ethyl-6-chrysenecarbaldehyde | HCID 13375390 | — |
| Reactant | 2-((6-Chrysenylmethyl)amino)-2-methyl-1,3-propanediol methanesulfonate | HCID 54096087 | — |
| Product | 2-(((12-Ethyl-6-chrysenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate | HCID 54456448 | — |
Reaction Steps
Using the reductive amination procedure outlined in 1C, 12-ethyl-6-chrysenecarbaldehyde (15A) and 2-amino-2-methyl-1,3-propanediol (Aldrich) gave 2-(((12-ethyl-6-chrysenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate mp 189°-192° (dec), (EtOH/Et2O), (C, H, N, S).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04810727 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-706463a2fdf34476a584f910aa9a37da |
| Source note | uspto-grants-1989_03 |