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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1193875Generated: November 1, 2026

Sodium → HCID 21270779, compound

https://huagongshe.com/reaction/1193875

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodiumHCID 5360545—
ReactantHCID 21270698HCID 21270698—
SolventIsopropanolHCID 3776—
ProductHCID 21270779HCID 21270779—

Reaction Steps

using isopropyl 2-chloro-5-[2-chloro-6-oxo-4-pentafluoroethyl-1(6H)-pyrimidinyl]-4-fluorobenzoate and sodium isopropylate in isopropanol there is obtained isopropyl 2-chloro-4-fluoro-5-[2-isopropoxy-6 -oxo-4-pentafluoroethyl-1(6H)-pyrimidinyl]-benzoate, 1H-NMR (CDCl3, 400 MHz): 7 83 ppm (d,1H), 7.39 ppm (d,1H), 6.64 ppm (s,1H), 5.34 ppm (m,1H), 5.27 ppm (m,1H), 1.39 ppm (d,3H), 1.38 ppm (d,3H), 1.28 ppm (d,3H), 1.27 ppm (d,3H);

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04812164
Source datasetuspto-grants-1989_03
ORD IDord-f88c7e908b5742558b9a0e0a0e14d379
Source noteuspto-grants-1989_03