Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 178514481 | HCID 178514481 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178514478 | HCID 178514478 | 78% |
Reaction Steps
2 g 6-azido-2,3-dihydroxyquinoxaline is suspended in 100 ml glacial acetic acid. To the suspension is added 16 ml fuming nitric acid at 24° C. The mixture is stirred at 24° C. for 4 h giving a precipitate of 1.9 g (78%) 6-azido-2,3-dihydroxy-7-nitroquinoxaline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04812458 |
|---|
| Source dataset | uspto-grants-1989_03 |
|---|
| ORD ID | ord-28d430d626b14d9d9172b67ad5e9ea59 |
|---|
| Source note | uspto-grants-1989_03 |
|---|
