HCID 13854275, compound → 2,2-Dimethyl-3-(6-phenoxypyridin-2-yl)methoxypropan-1-al

HRID 1194032Notes

Reaction equation

HRID 1194032 reaction equation
[CH3:1][C:2]([CH3:21])([CH2:5][O:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([O:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[N:9]=1)[CH2:3][OH:4]>C(OCC)C>[CH3:1][C:2]([CH3:21])([CH2:5][O:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([O:14][C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=2)[N:9]=1)[CH:3]=[O:4]

Participants

3

Reactant 1

HCID 13854275HCID 13854275, compound

Product 1

HCID 138542762,2-Dimethyl-3-(6-phenoxypyridin-2-yl)methoxypropan-1-al

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

2,2-Dimethyl-3-(6-phenoxypyridin-2-yl)methoxypropan-1-ol was reacted according to the procedure set out in Example 6. The crude product was subject to column chromatography on silica gel using petroleum ether (boiling range 40°-60° C.) containing 20% by volume diethylether as eluent, to give 2,2-dimethyl-3-(6-phenoxypyridin-2-yl)methoxypropan-1-al.

Sources & evidence

ORD record
ord-af3e8f6cf54d42e5bc964499fa48d15a
Source dataset
uspto-grants-1989_03
Patent number
US04812483

Reaction notes

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