Carbamate → HCID 45259199, compound

HRID 1194142Notes

Reaction equation

HRID 1194142 reaction equation
C(=O)([O-])N.[Cl:5][C:6]([O:8][C:9]1[CH:14]=[CH:13][C:12]([O:15][CH3:16])=[CH:11][CH:10]=1)=[O:7].[CH3:17][NH:18][CH2:19][CH2:20][N:21](C(C)(C)C)C(=O)[O-]>>[ClH:5].[CH3:16][O:15][C:12]1[CH:13]=[CH:14][C:9]([O:8][C:6](=[O:7])[N:18]([CH3:17])[CH2:19][CH2:20][NH2:21])=[CH:10][CH:11]=1

Participants

4

Reactant 3

HCID 276CarbamateHCID 82128Carbonochloridic acid, 4-methoxyphenyl esterHCID 19868745HCID 19868745, compound

Product 1

HCID 45259199HCID 45259199, compound

Procedure

This carbamate, m.p. 152.5°-154.5°, was prepared from 4-methoxyphenyl chloroformate and N-[2-(methylamino)ethyl]tert.-butylcarbamate by the procedure of Example 1.

Sources & evidence

ORD record
ord-868f472dd9b144d6a70b757b77b7c19a
Source dataset
uspto-grants-1989_03
Patent number
US04812590

Reaction notes

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