Carbamate → 122734-33-2

HRID 1194143Notes

Reaction equation

HRID 1194143 reaction equation
C(=O)([O-])N.[Cl:5][C:6]([O:8][C:9]1[CH:14]=[CH:13][C:12]([O:15][CH3:16])=[CH:11][CH:10]=1)=[O:7].[NH2:17][CH2:18][CH2:19][CH2:20][N:21](C(C)(C)C)C(=O)[O-]>>[ClH:5].[CH3:16][O:15][C:12]1[CH:13]=[CH:14][C:9]([O:8][C:6](=[O:7])[NH:17][CH2:18][CH2:19][CH2:20][NH2:21])=[CH:10][CH:11]=1

Participants

4

Reactant 3

HCID 276CarbamateHCID 82128Carbonochloridic acid, 4-methoxyphenyl esterHCID 86608743HCID 86608743, compound

Product 1

HCID 45263856122734-33-2

Procedure

This carbamate, m.p. 162°-165° soften at 110°, was prepared from 4-methoxyphenyl chloroformate and N-[3-aminopropyl]tert.-butylcarbamate by the procedure of Example 1.

Workup

  1. customsoften at 110°

Sources & evidence

ORD record
ord-198a140a456c45ec80ce052fd3db47e4
Source dataset
uspto-grants-1989_03
Patent number
US04812590

Reaction notes

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