Palmitoyl chloride → HCID 21269391, compound

HRID 1194274Notes

Reaction equation

HRID 1194274 reaction equation
[C:1](Cl)(=[O:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[NH:19]1[CH:23]=[N:22][CH:21]=[N:20]1>C(Cl)Cl>[C:1]([N:19]1[CH:23]=[N:22][CH:21]=[N:20]1)(=[O:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 8206Palmitoyl chlorideHCID 92571H-1,2,4-Triazole

Product 1

HCID 21269391HCID 21269391, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent2×

Procedure

Palmitoyl chloride is dissolved in methylene chloride and added dropwise to a solution of 2 equivalents of 1,2,4-triazole in methylene chloride, the mixture is stirred for some hours at room temperature and filtered, and the filtrate is used directly in the reaction.

Workup

  1. filtrationfiltered
  2. customthe filtrate is used directly in the reaction

Sources & evidence

ORD record
ord-e497f67dff8d45209cacf49d65551610
Source dataset
uspto-grants-1989_03
Patent number
US04814112

Reaction notes

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