HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → Ethylacrylate acrylic acid acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | Lauryl peroxide | HCID 76169 | — |
| Reactant | Butyl perbenzoate | HCID 83282 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | Ethylacrylate acrylic acid acrylonitrile | HCID 168852 | — |
Reaction Steps
this polymer material was produced by adding to 320g xylene at 100° C. the monomer solution and a catalyst solution over a period of 3 hours. The monomer solution contained 2.900g ethyl acrylate, 76g acrylonitrile, 76g acrylic acid and 3g laurylmercaptan. The catalyst solution contained 26g laurylperoxide and 7g butylperbenzoate in 273g of xylene. The material was highly viscous with comonomer proportions of 95:2.5:2.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814215 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-b49eff8d34704bb290fcc0074a7ddde4 |
| Source note | uspto-grants-1989_03 |