HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl chloride → HCID 21269524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl chloride | HCID 7850 | — |
| Reactant | HCID 21269561 | HCID 21269561 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21269524 | HCID 21269524 | — |
Reaction Steps
6.86 g (25 mmoles) of 5-phenylsulfinyl-benzimidazoline-2-thione and 4.9 ml (60 mmoles) of allylchloride are refluxed in 50 ml of ethanol for 24 hours. Then the reaction mixture is concentrated and the residue is crystallized from acetonitrile. The weight of the filtered endproduct is 7.68 g (87.55%). After recrystallization from ethanol it melts at 168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814329 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-e1b983678dfe4a3eb74d96d72c91aa8c |
| Source note | uspto-grants-1989_03 |