1-(triphenylmethyl)-1H-imidazole-4-carbaldehyde → HCID 21269997, compound

HRID 1194376Notes

Reaction equation

HRID 1194376 reaction equation
Br[C:2]1[C:7]([O:8][CH3:9])=[CH:6][CH:5]=[C:4]([CH2:10][O:11][CH3:12])[C:3]=1[O:13][CH3:14].[C:15]1([C:21]([C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)([C:29]2[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=2)[N:22]2[CH:26]=[C:25]([CH:27]=[O:28])[N:24]=[CH:23]2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH3:14][O:13][C:3]1[C:4]([CH2:10][O:11][CH3:12])=[CH:5][CH:6]=[C:7]([O:8][CH3:9])[C:2]=1[CH:27]([C:25]1[N:24]=[CH:23][N:22]([C:21]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)([C:29]2[CH:30]=[CH:31][CH:32]=[CH:33][CH:34]=2)[C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[CH:26]=1)[OH:28]

Participants

3

Reactant 2

HCID 6182331-(triphenylmethyl)-1H-imidazole-4-carbaldehydeHCID 14520331HCID 14520331, compound

Product 1

HCID 21269997HCID 21269997, compoundYield 48%

Procedure

Starting from 1-bromo-2,6-dimethoxy-3-methoxymethylbenzene and 1-triphenylmethyl-1H-imidazole-4-carboxaldehyde. The reaction product is purified by chromatography on silica and is present in the form of a glassy lac. Yield: 48% of theory.

Workup

  1. customThe reaction product is purified by chromatography on silica

Sources & evidence

ORD record
ord-6ffc884b3d924c74943d1107e4e7f1cd
Source dataset
uspto-grants-1989_03
Patent number
US04814343

Reaction notes

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