HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetic Acid → N-Phenylglycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetic Acid | HCID 300 | — |
| Reactant | Aniline | HCID 6115 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-Phenylglycine | HCID 66025 | — |
Reaction Steps
475 g of chloracetic acid (5 moles) are heated with 930 g aniline (10 moles) in 2 l water for 1.5 h to 100° C. After cooling, the N-phenylglycine formed is suctioned off and washed with water. Yield is 468 g (=62% with respect to the chloracetic acid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814345 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-cc7da110d22d48a6b27281352d6976ee |
| Source note | uspto-grants-1989_03 |