Diethyl ether ethanol → HCID 53637278, compound

HRID 1194432Notes

Reaction equation

HRID 1194432 reaction equation
C(O)C.CCOCC.[Br-].[CH3:10][N:11]([CH3:49])[C:12]1[CH:48]=[CH:47][C:15]([CH:16]=[N:17][N:18]2[CH:22]=[CH:21][N+:20](CC(C3C=CC(N(C)C)=CC=3)=O)=[C:19]2[C:35]2[CH:40]=[C:39]([O:41][CH3:42])[C:38]([O:43][CH3:44])=[C:37]([O:45][CH3:46])[CH:36]=2)=[CH:14][CH:13]=1.C(#N)C>>[CH3:49][N:11]([CH3:10])[C:12]1[CH:48]=[CH:47][C:15]([CH:16]=[N:17][N:18]2[CH:22]=[CH:21][N:20]=[C:19]2[C:35]2[CH:36]=[C:37]([O:45][CH3:46])[C:38]([O:43][CH3:44])=[C:39]([O:41][CH3:42])[CH:40]=2)=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 21585056Diethyl ether ethanolHCID 73867530HCID 73867530, compound

Product 1

HCID 53637278HCID 53637278, compound

Procedure

In an analogous manner, from 1-[[p-(dimethylamino)benzylidene]amino]-2-(3,4,5-trimethoxyphenyl)imidazole, there is obtained after 2 days at 50° in acetonitrile 3-[[p-(dimethylamino)benzylidene]amino]-1-[p-(dimethylamino)phenacyl]-2-(3,4,5-trimethoxyphenyl)imidazolium bromide of melting point 232° (ethanol/ether).

Sources & evidence

ORD record
ord-79af380494e747ccbd2a69b5aa15ce10
Source dataset
uspto-grants-1989_03
Patent number
US04814332

Reaction notes

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