Ethylene carbonate → HCID 14950291, compound

Participants

Reaction Conditions

Reaction Steps

90.7 grams (1.03 moles) of ethylene carbonate were placed in a flask, melted and stirred at about 50° C. 104.2 grams (1.03 moles) of n-hexylamine were then added drop wise over a 11/2 hour period to the flask at a rate sufficient to maintain the flask contents at 60° to 70° C. The flask contents were held at 80° C. for an additional 51/2 hours and then allowed to cool overnight. Infrared and NMR analyses of the resultant product were consistent with the proposed structure.

Provenance & Evidence