Ethylene carbonate → HCID 19899276, compound

Participants

Reaction Conditions

Reaction Steps

135 grams (1.5 moles, 98% pure) of ethylene carbonate were charged to a flask and heated to approximately 50° C. to melt it. 198 grams (1.5 moles, 98% pure) of 2-ethyl-1-hexylamine were charged to a dropping funnel and fed drop-wise to the stirred flask contents at a rate sufficient to maintain the reaction mixture at 70° C. during the addition. The resulting mixture was heated at 95° C. for an additional 10 hours. Infrared analysis of the resultant product was consistent with the proposed structure.

Provenance & Evidence