Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1194493Generated: October 31, 2026

Methanol → HCID 131714282, compound

https://huagongshe.com/reaction/1194493

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSilver NitrateHCID 24470—
ReactantHCID 13303848HCID 13303848—
SolventPyridineHCID 1049—
ProductHCID 131714282HCID 131714282—

Reaction Conditions

Temperature20 °C

Reaction Steps

To a 50 ml flask equipped with a nitrogen atmosphere add 10 ml of methanol and 460 mg of (3S,4R)-1-(allyloxycarbonylmethyl)-3-(1-hydroxyethyl)-4-(triphenylmethylthio)azetidin-2-one. To this system add 160 mg silver nitrate and 0.15 ml of pyridine. Stir the system at 20° C. for 1 hour. Stop the reaction and remove the methanol by stripping to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04814442
Source datasetuspto-grants-1989_03
ORD IDord-7861a79f32ad4b8e8d89cf976e876cff
Source noteuspto-grants-1989_03