HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → P-Toluic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | 4-Methylbenzaldehyde | HCID 7725 | — |
| Reactant | Calcium hypochlorite | HCID 24504 | — |
| Product | P-Toluic Acid | HCID 7470 | — |
Reaction Steps
In the like manner as Example 1, 23.6 g of p-methylbenzaldehyde as an aldehyde and 3 g of phosphoric acid were used. The oxidation was done by using 23 g of calcium hypochlorite at temperatures of -5° to -3° C., which was followed by refining to obtain p-methylbenzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814494 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-6654397f858549979f52f39e4f9e4ced |
| Source note | uspto-grants-1989_03 |