化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → 2,6-Diacetoxynaphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | 2,6-Dihydroxynaphthalene | HCID 93552 | — |
| 生成物 | 2,6-Diacetoxynaphthalene | HCID 594930 | 93% |
反応手順
Subsequently, 45 g of the thus obtained 2,6-dihydroxynaphthalene were acetylated with 23 g of acetic acid and 61 g of acetic anhydride in the same manner as in Example 7 to obtain 60.6 g of 2,6-diacetoxynaphthalene of the purity of 99.85% (by DSC) in a yield of 93.0%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04814521 |
| 出典データセット | uspto-grants-1989_03 |
| ORD ID | ord-125a9af4a1244cbc9c74452cd8c293f0 |
| 出典メモ | uspto-grants-1989_03 |