HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Octyloxybenzoyl chloride | HCID 2760250 | — |
Reaction Steps
2.78 g of 4-octyloxybenzoic acid was added to 10 ml of benzene, and under stirring at room temperature, 2.36 g of PCl5 was added little by little. The mixture was then heated under reflux for 4 hours. Thereafter, the solvent was distilled off to obtain 4-octyloxybenzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816178 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-f9a4d6e25c00415cafdbea296e105925 |
| Source note | uspto-grants-1989_03 |