HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 53878260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 19817367 | HCID 19817367 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53878260 | HCID 53878260 | — |
Reaction Steps
3.29 g of 4-heptylbiphenylcarboxylic acid was added to 10 ml of benzene, and 2.36 g of PCl5 was added little by little under stirring at room temperature, followed by 4 hours of heat-refluxing. Thereafter, the solvent was distilled off to obtain 4-heptylbiphenylcarboxylic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816178 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-1f71b2e8f6994e378c101b2088a977c1 |
| Source note | uspto-grants-1989_03 |