HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4'-(Phenylmethoxy)(1,1'-biphenyl)-4-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4'-(Benzyloxy)[1,1'-biphenyl]-4-carboxylic acid | HCID 14744793 | — |
| Product | Thionyl Chloride | HCID 24386 | — |
| Product | 4'-(Phenylmethoxy)(1,1'-biphenyl)-4-carbonyl chloride | HCID 15084904 | 154.9% |
Reaction Steps
Thionyl chloride (140 g, 1.18 mol) was added to 4'-benzyloxybiphenyl-4-carboxylic acid (300 g, 0.98 mol), followed by refluxing the mixture for about 2 hours, thereafter removing excess thionyl chloride under reduced pressure to obtain 4'-benzyloxybiphenyl-4-carboxylic chloride (295 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816181 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-c56cee0c4f334acc92c8cd65080e1f34 |
| Source note | uspto-grants-1989_03 |