HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Benzyloxy)benzoic acid → 4-Benzyloxybenzoylchloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Benzyloxy)benzoic acid | HCID 73880 | — |
| Reactant | HCID 21248649 | HCID 21248649 | — |
| Product | Thionyl Chloride | HCID 24386 | — |
| Product | 4-Benzyloxybenzoylchloride | HCID 3766410 | 144.3% |
Reaction Steps
Preparation of optically active 4-(1-methylheptyloxycarbonyl)phenol Thionyl chloride (140 g, 1.18 mol) was added to 4-benzyloxybenzoic acid (220 g, 0.98 mol), followed by refluxing the mixture for about 2 hours, thereafter removing excess thionyl chloride under reduced pressure to obtain 4-benzyloxybenzoic chloride (210 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816181 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-ec3081767d2f4e419a3e4a6238a00028 |
| Source note | uspto-grants-1989_03 |