Carbon Dioxide → HCID 13377158, compound

HRID 1194683Notes

Reaction equation

HRID 1194683 reaction equation
[C:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[CH:7]=[C:6]([N+:13]([O-:15])=[O:14])[C:5]=1[S:16][CH2:17]C(O)=O)(=O)[CH3:2].C(=O)=O>C(O)(=O)CC>[CH3:2][C:1]1[C:4]2[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[CH:7]=[C:6]([N+:13]([O-:15])=[O:14])[C:5]=2[S:16][CH:17]=1

Participants

4

Reactant 2

HCID 280Carbon DioxideHCID 13377157HCID 13377157, compound

Product 1

HCID 13377158HCID 13377158, compound

Reagents, catalysts & solvents 1

HCID 1032Propionic AcidSolvent

Procedure

A solution of 0.8 mole of (2-acetyl-4,6-dinitrophenylthio)acetic acid in 1 liter of propionic acid is heated at the boiling point until the evolution of CO2 has ended (about 4 hours).

Workup

  1. custom(about 4 hours)

Sources & evidence

ORD record
ord-541379cbee2d4aa4ab2a588e9814edd0
Source dataset
uspto-grants-1989_03
Patent number
US04816461

Reaction notes

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