HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 14407250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 14407249 | HCID 14407249 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14407250 | HCID 14407250 | 70.7% |
Reaction Steps
A solution of 3-chloro-5-(trichlorovinyl)benzyl bromide (3.57 g) and sodium azide (813 mg) in 50 ml of ethanol was heated at reflux for 30 minutes. The reaction was then concentrated and the residue chromatographed on silica gel with petroleum ether as eluant to afford 2.24 g of pure 3-chloro-5-(trichlorovinyl)benzyl azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816469 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-6452cccefdaa4a42b1a82e1254adb520 |
| Source note | uspto-grants-1989_03 |