HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 23036226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 23036221 | HCID 23036221 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23036226 | HCID 23036226 | 95.6% |
Reaction Steps
A solution of 3-methyl-5-(trichlorovinyl)benzyl bromide (3.14 g) and sodium azide (1.0 g) in 25 ml of ethanol was heated at reflux for 2 hours. The reaction mixture was concentrated under reduced pressure and the resulting oil triturated with 50 ml of hexane. The mixture was filtered and the filtrate concentrated to give 2.64 g of azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816469 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-27f4210082774cc9a8d40bdda56c99cf |
| Source note | uspto-grants-1989_03 |