HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 23036209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 23036227 | HCID 23036227 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23036209 | HCID 23036209 | — |
Reaction Steps
A solution of 3-fluoro-5-(trichlorovinyl)benzyl bromide (3.18 g) and sodium azide (0.975 g) in 25 ml of ethanol is heated at reflux for 2 hours. The reaction mixture is concentrated and the residue triturated with 50 ml of hexane. The mixture is filtered and the filtrate concentrated to give the desired azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816469 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-66468236b01a411e8800c2b762dab69c |
| Source note | uspto-grants-1989_03 |