HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → Benzyl azide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Benzyl azide | HCID 12152 | 144.9% |
Reaction Steps
The reaction of this crude benzyl bromide (6.7 g) and sodium azide (1.92 g) in ethanol (90 ml) at reflux as in Example 33 yielded 5.7 g of crude benzyl azide. Chromatography on silica gel afforded 3.98 g of pure 4-(trichlorovinyl)benzyl azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816469 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-c33647f7c454415ea45d2f8708fe5b34 |
| Source note | uspto-grants-1989_03 |