HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 21268692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21268696 | HCID 21268696 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21268692 | HCID 21268692 | — |
Reaction Steps
A solution of 7-(4-methylthiobenzyl)benzofuran-5-ylacetic acid (10 g), dichloromethane (100 ml), thionyl chloride (10.0 ml) and dimethylformamide (0.2 ml) was stirred at room temperature for 6 hours. The solvent was then evaporated to give a residue which contained the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816473 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-10e25f488f3948d9a540b0130bfa6522 |
| Source note | uspto-grants-1989_03 |