Bromine → HCID 21249071, compound

HRID 1194920Notes

Reaction equation

HRID 1194920 reaction equation
[Cl:1][C:2]1[CH:19]=[CH:18][CH:17]=[C:16]([Cl:20])[C:3]=1[CH2:4][O:5]/[N:6]=[C:7](/[C:13](=[O:15])[CH3:14])\[C:8]([O:10][CH2:11][CH3:12])=[O:9].[Br:21]Br>>[Br:21][CH2:14][C:13](=[O:15])/[C:7](=[N:6]/[O:5][CH2:4][C:3]1[C:2]([Cl:1])=[CH:19][CH:18]=[CH:17][C:16]=1[Cl:20])/[C:8]([O:10][CH2:11][CH3:12])=[O:9]

Participants

3

Reactant 2

HCID 24408BromineHCID 140352853HCID 140352853, compound

Product 1

HCID 21249071HCID 21249071, compound

Procedure

Ethyl (Z)-2-(2,6-dichlorobenzyloxyimino)-3-oxobutyrate (5.8 g) was reacted with bromine (0.94 ml) as described in Example 4c to give the title compound (7.2 g), δH (CDCl3) 1.31 (3H, t), 4.35 (2H, s), 4.45 (2H, q), 5.73 (2H, s), and 7.43 (3H, m).

Sources & evidence

ORD record
ord-68dfac49ae5843f392d6324294a1854f
Source dataset
uspto-grants-1989_03
Patent number
US04816452

Reaction notes

Loading…