Thioglycerol → HCID 88627743, compound

Participants

Reaction Steps

Ethyl 2-(2-aminothiazol-4-yl)-(Z)-2-(2,6-dichlorobenzyloxyimino)acetate (4.8 g) was hydrolysed with aqueous sodium hydroxide (1N, 25.6 ml) in ethanol (40 ml), acetone (20 ml) as described in Example 4e to give the title compound (1.9 g), νmax (KBr) 3123 (br), 1610 (br), and 992 cm-1, δH [(CD3)2SO]5.32 (2H, s), 6.81 (1H, s), 7.17 (2H, br s), and 7.44 (3H, m), [Mass spectrum: +ve ion (thioglycerol) MH+ (346)].

Provenance & Evidence