HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → Aluminum tri-iso-propoxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Aluminum | HCID 5359268 | — |
| Product | Aluminum tri-iso-propoxide | HCID 16685055 | 90% |
Reaction Steps
360 g anhydrous isopropanol, 0.0959 g mercuric salt and 13.5 g metallic aluminium scraps was refluxed at 83°-90° C. for 2-8 hours, evaporated off excess isopropand under normal pressure, triisopropoxyl aluminum was obtained by collecting distillation fraction of 110°-200° C. under reduced pressure of 1-10 mmHg. yield 90-100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816594 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-c87c065aee1247c48e7be847b22c70b4 |
| Source note | uspto-grants-1989_03 |