HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 18608977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Lysergol | HCID 14987 | — |
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Product | HCID 18608977 | HCID 18608977 | — |
Reaction Steps
1 g of lysergol is halogenated according to the process of Example 1, except that 1.7 g of trimethylchlorosilane are used instead of trimethylbromosilane. The product is isolated as described in Example 1. The yield of the title compound is 0.73 g (0.0025347 mole, 64.4%), m.p.: 207° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816587 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-3b3cee83e4b44f6ab32f2d558d4f2303 |
| Source note | uspto-grants-1989_03 |