Thionyl Chloride → HCID 54224112, compound

HRID 1195100Notes

Reaction equation

HRID 1195100 reaction equation
[CH2:1]([C:10]1[CH:11]=[N:12][C:13]([C:16]2[CH:24]=[CH:23][C:19]([C:20](O)=[O:21])=[CH:18][CH:17]=2)=[N:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].S(Cl)([Cl:27])=O>>[CH2:1]([C:10]1[CH:11]=[N:12][C:13]([C:16]2[CH:24]=[CH:23][C:19]([C:20]([Cl:27])=[O:21])=[CH:18][CH:17]=2)=[N:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 190284734-(5-Nonylpyrimidin-2-yl)benzoic acid

Product 1

HCID 54224112HCID 54224112, compound

Procedure

4-(5-n-Nonylpyrimidine-2-yl)benzoic acid (1.63 g) was heated together with excess thionyl chloride for 8 hours under reflux and thereafter, unaltered thionyl chloride was distilled off to obtain 4-(5-n-nonylpyrimidine-2-yl)benzoic acid chloride.

Workup

  1. temperatureunder reflux
  2. distillationunaltered thionyl chloride was distilled off

Sources & evidence

ORD record
ord-76d6be173910499688c3f328772855ef
Source dataset
uspto-grants-1992_05
Patent number
US05110496

Reaction notes

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