Thionyl Chloride → HCID 54001263, compound

HRID 1195107Notes

Reaction equation

HRID 1195107 reaction equation
[CH2:1]([O:10][C:11]1[CH:12]=[N:13][C:14]([C:17]2[CH:25]=[CH:24][C:20]([C:21](O)=[O:22])=[CH:19][CH:18]=2)=[N:15][CH:16]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].S(Cl)([Cl:28])=O>>[CH2:1]([O:10][C:11]1[CH:12]=[N:13][C:14]([C:17]2[CH:25]=[CH:24][C:20]([C:21]([Cl:28])=[O:22])=[CH:19][CH:18]=2)=[N:15][CH:16]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 53902994HCID 53902994, compound

Product 1

HCID 54001263HCID 54001263, compound

Procedure

4-(5-n-Nonyloxylpyrimidine-2-yl)benzoic acid (1.78 g) was heated together with excess thionyl chloride for 8 hours under reflux and thereafter, unaltered thionyl chloride was distilled off to obtain 4-(5-n-nonyloxypyrimidine-2-yl)benzoic acid chloride.

Workup

  1. temperatureunder reflux
  2. distillationunaltered thionyl chloride was distilled off

Sources & evidence

ORD record
ord-7e271a7432434ad482539bf4beb125df
Source dataset
uspto-grants-1992_05
Patent number
US05110496

Reaction notes

Loading…