Thionyl Chloride → HCID 54508141, compound

HRID 1195111Notes

Reaction equation

HRID 1195111 reaction equation
[CH2:1]([O:12][C:13]1[CH:14]=[N:15][C:16]([C:19]2[CH:27]=[CH:26][C:22]([C:23](O)=[O:24])=[CH:21][CH:20]=2)=[N:17][CH:18]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].S(Cl)([Cl:30])=O>>[CH2:1]([O:12][C:13]1[CH:14]=[N:15][C:16]([C:19]2[CH:27]=[CH:26][C:22]([C:23]([Cl:30])=[O:24])=[CH:21][CH:20]=2)=[N:17][CH:18]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 53709528HCID 53709528, compound

Product 1

HCID 54508141HCID 54508141, compound

Procedure

4-(5-n-Undecyloxypyrimidine-2-yl)benzoic acid (1.86 g) was heated together with excess thionyl chloride for 8 hours under reflux and thereafter, unaltered thionyl chloride was distilled off to obtain 4-(5-n-undecyloxypyrimidine-2-yl)benzoic acid chloride.

Workup

  1. temperatureunder reflux
  2. distillationunaltered thionyl chloride was distilled off

Sources & evidence

ORD record
ord-1f9afcfecfbd41988e0398383792b673
Source dataset
uspto-grants-1992_05
Patent number
US05110496

Reaction notes

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