Thionyl Chloride → HCID 54366973, compound

HRID 1195119Notes

Reaction equation

HRID 1195119 reaction equation
[CH2:1]([C:12]1[CH:17]=[CH:16][C:15]([C:18]2[N:23]=[CH:22][C:21]([C:24]([OH:26])=O)=[CH:20][N:19]=2)=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].S(Cl)([Cl:29])=O>>[CH2:1]([C:12]1[CH:17]=[CH:16][C:15]([C:18]2[N:23]=[CH:22][C:21]([C:24]([Cl:29])=[O:26])=[CH:20][N:19]=2)=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 53791351HCID 53791351, compound

Product 1

HCID 54366973HCID 54366973, compound

Procedure

2-(4-n-Undecylphenyl)pyrimidine-5-yl-carboxylic acid (1.7 g) was heated together with excess thionyl chloride for 4 hours under reflux and thereafter, unaltered thionyl chloride was distilled off to obtain 2-(4-n-undecylphenyl)pyrimidine-5-yl-carboxylic acid chloride.

Workup

  1. temperatureunder reflux
  2. distillationunaltered thionyl chloride was distilled off

Sources & evidence

ORD record
ord-f438751b86c3449896ff13300d5105a3
Source dataset
uspto-grants-1992_05
Patent number
US05110496

Reaction notes

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