HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53864583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 54137794 | HCID 54137794 | — |
| Product | HCID 53864583 | HCID 53864583 | — |
Reaction Steps
3-Fluoro-4-(5-n-octyloxypyrimidine-2-yl)benzoic acid (1.60 g) was heated together with excess thionyl chloride for 8 hours under reflux and thereafter, unaltered thionyl chloride was distilled off to obtain 3-fluoro-4-(5-n-octyloxypyrimidine-2-yl)benzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110496 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-f89ca3d473ea49cfab66d5746b4f30a2 |
| Source note | uspto-grants-1992_05 |