HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichloroaniline → 4-Chloro-N-([(3,4-dichlorophenyl)amino]carbonyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichloroaniline | HCID 7257 | — |
| Reactant | 4-Chlorobenzenesulfonyl isocyanate | HCID 138587 | — |
| Product | 4-Chloro-N-([(3,4-dichlorophenyl)amino]carbonyl)benzenesulfonamide | HCID 14480020 | 91.7% |
Reaction Steps
Following the procedure of Example 1, 5.04 g of 4-chlorobenzenesulfonyl isocyanate and 3.85 g of 3,4-dichloroaniline were allowed to react providing 8.06 g of the desired title product, m.p. 195-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110830 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-9c7a59182a664352a37105d828abbf63 |
| Source note | uspto-grants-1992_05 |