HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1195239Generated: October 30, 2026
HCID 19819013, compound → HCID 19819021, compound
https://huagongshe.com/reaction/1195239
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 19819013 | HCID 19819013 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 19819021 | HCID 19819021 | 56% |
Reaction Steps
A solution of dicyclopropylmethanimine hydrobromide (1.00 g, 5.26 mmol) in 6.0 ml of dimethyl sulfoxide was heated with stirring at 100° C. for 1 hour. The solvent was distilled out in vacuo and of isobutyl alcohol (8 ml) was added to the residue. Precipitated crystals was obtained and dried in vacuo to afford 0.56 g (Yield: 56%) of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05110945 |
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| Source dataset | uspto-grants-1992_05 |
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| ORD ID | ord-33811c3787354e279c0d15ff08a02205 |
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| Source note | uspto-grants-1992_05 |
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