HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 15611848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 2-Dimethylaminoethyl benzoate | HCID 75158 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15611848 | HCID 15611848 | — |
Reaction Steps
A solution of 57.96 g (0.30 mol) of 2-(N,N-dimethylamino)ethyl benzoate (prepared as described in Example 2), 37.98 g (0.30 mol) of benzyl chloride and 500 ml of acetonitrile was heated at reflux for 2 hours. The reaction mixture was concentrated to a white solid which was then washed with ether and recrystallized from acetonitrile. The yield of product was 69.0 g; mp=164°-6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110977 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-12a7f1200ede4620866295415c0bd85a |
| Source note | uspto-grants-1992_05 |