Benzyl Chloride → HCID 19774311, compound

Participants

Reaction Steps

A solution of 28.5 g (0.084 mol) of N,N-bis(2-cyclohexanoyloxyethyl)methylamine (prepared as described in Example 22), 10.63 g (0.084 mol) of benzyl chloride and 200 ml of acetonitrile was heated at reflux for 2.5 hours and concentrated to an oil. Ether was added to the oil which induced crystallization. The white solid was collected, washed two times with ether and recrystallized from 2-butanone. The yield of product was 8.3 g; mp=143.5°-4.5° C.

Provenance & Evidence