HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 53731305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 14832329 | HCID 14832329 | — |
| Product | HCID 53731305 | HCID 53731305 | — |
Reaction Steps
146 g (0.3 mol) of 2-(4-carboxyphenyl)-2-[4-(3-nitrophenoxy)phenyl]hexafluoropropane were suspended in 714 g of thionyl chloride, 1 cm3 of dimethylformamide was added, and the mixture was refluxed till evolution of gas was no longer observed. The thionyl chloride was removed by distillation, and the residue was recrystallized from acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110983 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-5d574b0d7def43b38dbb6df7260e59e2 |
| Source note | uspto-grants-1992_05 |