HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-Bromoundecanoic acid → Undecanoyl chloride, 11-bromo-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-Bromoundecanoic acid | HCID 17812 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Undecanoyl chloride, 11-bromo- | HCID 85202 | — |
Reaction Steps
50 g of 11-bromoundecanoic acid was heat-refluxed with 90.0 of thionyl chloride for 2 hours. Then, unreacted thionyl chloride was distilled away, and the residue was vacuum-distilled, to obtain 11- bromoundecanoic acid chloride. Said product was stirred with 37.6 g of anhydrous aluminum chloride in methylene chloride so as not to be 5° C. or more, to obtain a methlene chloride solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110964 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-d71b8e09ee664b50951d02b93c5dfec1 |
| Source note | uspto-grants-1992_05 |