HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1195466Generated: November 2, 2026
Pyrophosphoric acid → HCID 178443540, compound
https://huagongshe.com/reaction/1195466
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyrophosphoric acid | HCID 1023 | — |
| Reactant | Sebacic Acid | HCID 5192 | — |
| Reactant | Bis(eta-cyclopentadienyl) iron | HCID 7611 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178443540 | HCID 178443540 | 60% |
Reaction Steps
0.67 g of sebacic acid, 1.0 ml of triethylamine and 2 ml of phosphorus oxychloride with 40 ml of methylene chloride were added and stirred at 0° C. for 30 minutes, and then 60 ml of pyrophosphoric acid and 6.0 g of ferrocene were added, and the resulting mixture was heat-refluxed. Subsequently, the same procedure as in Example 7 was conducted, to obtain a ferrocenoylnonanoic acid in an amount of 2.22 g and in a yield of 60.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05110964 |
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| Source dataset | uspto-grants-1992_05 |
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| ORD ID | ord-c898a3de70cf4c9d819555a382093623 |
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| Source note | uspto-grants-1992_05 |
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