HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 54546446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 1-(3,3-Dimethylbut-1-yn-1-yl)-4-methylbenzene | HCID 12861407 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 54546446 | HCID 54546446 | — |
Reaction Steps
3.35 g of 4-(3,3-Dimethyl-1-butynyl)toluene, 3.47 g of N-bromosuccinimide and 100 mg of dibenzoylperoxide in 50 ml of carbon tetrachloride are refluxed for 8 hours. The mixture is filtered and the solvent removed under vacuum. The pure product is obtained as an oil following chromatography over silica gel using hexane as an eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112851 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-4f9d2715ecc5465ba1a0ff39eadca18a |
| Source note | uspto-grants-1992_05 |