p-Toluidine → HCID 86745782, compound

Participants

Reaction Steps

The reaction between 4-methylaniline (1.61 g, 15 mmol) and ethenesulfonyl fluoride (2.18 g, 19 mmol) was carried out in DMF (30 mL) at ambient temperature for 2.5 hours as described in Example 16. There was obtained a tan residue which was crystallized from ether/hexane to afford the title compound as a tan solid (1.12 g 34% yield), mp 61°-65° C.

Provenance & Evidence