HuagongsheHuagongshe Chemistry Print Report · For research reference only
3',4',5'-Trimethoxyacetophenone → 3-(3-Methoxy-4-hydroxy-5-trifluoromethylphenyl)-1-(3,4,5-trimethoxyphenyl)prop-2-en-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3',4',5'-Trimethoxyacetophenone | HCID 14345 | — |
| Reactant | 4-Hydroxy-3-methoxy-5-(trifluoromethyl)benzaldehyde | HCID 19389199 | — |
| Product | 3-(3-Methoxy-4-hydroxy-5-trifluoromethylphenyl)-1-(3,4,5-trimethoxyphenyl)prop-2-en-1-one | HCID 54374357 | — |
Reaction Steps
The procedure described in Example 8 was repeated using 2.2 g of 3-methoxy-4-hydroxy-5-trifluoromethylbenzaldehyde and 2.1 g of 3',4',5'-trimethoxyacetophenone. Yield 2.6 g (61%), m.p. 190°-192° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112861 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-87df3a8906e841bda9bf39c4a6ce17c5 |
| Source note | uspto-grants-1992_05 |