HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Chloride → Anthraquinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Cyanuric chloride | HCID 7954 | — |
| Reactant | 1-Amino-2-carboxy-4-(3'-amino-4'-sulfophenylthio)anthraquinone | HCID 14876418 | — |
| Product | Anthraquinone | HCID 6780 | — |
Reaction Steps
1-Amino-2-carboxy-4-(3'-amino-4'-sulfophenylthio)anthraquinone (9.4 parts) and cyanuric chloride (3.7 parts) were subjected to condensation reaction in an aqueous medium in a usual manner, followed by condensation reaction with 1-aminobenzene-3-β-sulfatoethylsulfone (5.6 parts) at 20° to 40° C. under a weak acid condition. Thereafter, salting out of the reaction mixture with sodium chloride gave an anthraquinone compound of the following formula (free acid form). ##STR270##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112971 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-b080e49e3789492fb3ecb4299390ce54 |
| Source note | uspto-grants-1992_05 |