Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1196295Generated: October 27, 2026

Dicyclohexylcarbodiimide → HCID 178462154, compound

https://huagongshe.com/reaction/1196295

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDicyclohexylcarbodiimideHCID 10868—
ReactantBenzyloxycarbonyl-asparagineHCID 75314—
Reactant1-HydroxybenzotriazoleHCID 75771—
ReactantHydrogen chloride-ethyl acetateHCID 21866389—
ReactantHCID 178462202HCID 178462202—
ProductHCID 178462154HCID 178462154—

Reaction Steps

The desired compound was prepared from 2.9 g of Boc-Ala-Pro-Arg(NO2)-OBzl, 15 ml of 4N HCl-AcOEt, 1.4 g of Z-Asn-OH, 1.0 g of HOBt and 1.1 g of DCC in the same manner as in Example 7-(3).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05112947
Source datasetuspto-grants-1992_05
ORD IDord-5637d9363cfa4f14a3f6f08519974df1
Source noteuspto-grants-1992_05