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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1196299Generated: October 30, 2026

Dicyclohexylcarbodiimide → HCID 178512174, compound

https://huagongshe.com/reaction/1196299

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDicyclohexylcarbodiimideHCID 10868—
ReactantBenzyloxycarbonyl-asparagineHCID 75314—
Reactant1-HydroxybenzotriazoleHCID 75771—
ReactantHCID 178454226HCID 178454226—
SolventHydrogen chloride-ethyl acetateHCID 21866389—
ProductHCID 178512174HCID 178512174—

Reaction Steps

The desired compound was prepared from 3.0 g of Boc-Ser(Bzl)-D-Pro-Arg(NO2)-OBzl, 10 ml of 4N HCl-AcOEt, 1.2 g of Z-Asn-OH, 0.9 g of HOBt and 0.95 g of DCC in the same manner as in Example 7-(3).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05112947
Source datasetuspto-grants-1992_05
ORD IDord-a934fb018c084778814f4aebeae3ee16
Source noteuspto-grants-1992_05